| Problem |
Possible Cause |
Solution |
| Low RNA yield |
- Initial sample mass too large.
|
- The MagneSil*
Total RNA mini-Isolation System is optimized
for purification from =1 × 105 cells, =2mg tissue
lysate in 100µl, or =20µl whole blood. Exceeding
these limits will significantly reduce both yield
and concentration of the purifed RNA and will
cause excessive clumping of MagneSil* RNA
Paramagnetic Particles, making handling of the
particles difficult.
|
|
| Low RNA yield |
- Use of sample lysate that has been stored at
?20°C or ?70°C. Lysate samples that have been
frozen may have a decreased amount of total
RNA.
|
- For optimal performance, purify the total
RNA as soon as the lysate is prepared.
|
|
| Low RNA yield |
- Sample lysates have undergone multiple freezethaw
cycles. Samples that have been frozen and
thawed repeatedly will have some RNA
degradation.
|
- Use fresh samples whenever
possible.
|
|
| Low RNA yield |
- Tissue culture cells low in total RNA. The yield
of total RNA may vary depending on the sample
type.
|
- If total RNA yields are low, increase the
amount of starting material processed.
|
|
| Low RNA yield |
- RNA Lysis Buffer not added to tissue lysates.
|
- Make sure that RNA Lysis Buffer is added to all
sample lysates.
|
|
| Low RNA yield |
- Steps not followed correctly, or the wrong
reagents were used.
|
- Use the MagneSil* Total
RNA mini-Isolation System reagents in the order
specified. This ensures that the RNA remains
bound to the MagneSil* RNA PMPs during the
purification process.
|
|
| Low RNA yield |
- Ethanol not added to DNase Stop Solution.
|
- Ensure that ethanol is added to the DNase Stop
Solution. See Section IV.A.
|
|
| Low RNA yield |
- Incorrect concentration of ethanol wash. Ethanol
concentrations lower than 90% will result in
reduced yields.
|
- Make 90% ethanol wash solution
fresh before each purification.
|
|
| Low RNA yield |
- Failure to resuspend MagneSil* RNA PMPs in
reagent bottle.
|
- Thoroughly resuspend MagneSil*
RNA PMPs in the reagent bottle before
dispensing to the sample processing plate to
ensure even distribution of particles.
|
|
| Low RNA yield |
- Inaccurate dispensing of MagneSil* RNA PMPs.
The volumes of MagneSil* RNA PMPs used in
the protocol are optimized for yield and purity
of RNA.g
|
- Use of 25% greater than or less than the
recommended amount will result in decreased
yield (e.g., purification from 1 × 105 cultured
cells requires 30µl of MagneSil* RNA PMPs; no
less than 22.5µl and no more than 37.5µl of
particles should be used per isolation.)
|
|
| DNA contamination |
- DNase Solution not prepared correctly.
|
- For each
plate purification 5.2ml Yellow Core Buffer,
575µl MnCl2 and 275µl of DNase I are mixed to
make a DNase Solution.
|
|
| DNA contamination |
- Insufficient incubation with DNase Solution.
|
- Incubate DNase Solution for at least 10 minutes.
DNase incubation time can be lengthened up to
20 minutes.
|
|
| DNA contamination |
- DNase Solution stored or frozen before use.
|
- Make DNase Solution fresh before each use. It
cannot be prepared and then stored.
|
|
| MagneSil* RNA PMPs clump |
- Too much sample material used.
|
- MagneSil* RNA
mini-Isolation System input limitations are
=1 × 105 cells, =2mg tissue lysate in 100µl
volume and =20µl whole blood
|
|
| MagneSil* RNA PMPs clump |
|
- If the lysate is too
viscous, dilute with RNA Lysis Buffer until it
becomes easier to pipette.
|
|
| MagneSil* RNA PMPs clump |
|
- Vigorously mix during wash
and incubation steps to resuspend the
MagneSil* RNA PMPs.
|
|
| RNA degradation |
- RNase introduced during purification/handling.
|
- Use RNase-free plastic- or glassware during the
purification process. Use filter tips during all
pipetting steps. Wear gloves at all times. RNases
introduced after elution will degrade RNA.
|
|
* All trademarks are the property of their respective owners. Where applicable,
the PCR process is covered by patents owned by Roche Molecular Systems,
Inc., and F. Hoffman-LaRoche, Ltd.